首页> 外文会议>International Conference on Applied Sciences >Ultrasonic-assisted chemical reduction synthesis and structural characterization of copper nanoparticles
【24h】

Ultrasonic-assisted chemical reduction synthesis and structural characterization of copper nanoparticles

机译:超声波辅助化学还原合成及铜纳米粒子的结构表征

获取原文

摘要

Copper nanoparticles, due to their special properties, small dimensions and low-cost preparation, have many potential applications such as in optical, electronics, catalysis, sensors, antibacterial agents. In this study, copper nanoparticles were synthesized by chemical reduction method with different conditions in order to investigate the optimum conditions which gave the smallest (particle diameter) dimensions. The synthesis step used copper (II) acetate salt as precursor, ascorbic acid as reducing agent, glycerin and polyvinylpyrrolidone (PVP) as protector and stabilizer. The assistance of ultrasonic was were considered as the significant factor affecting the size of the synthesized particles. The results showed that the copper nanoparticles have been successfully synthesized with the diameter as small as 20-40 nm and the conditions of ultrasonic waves were 48 kHz of frequency, 20 minutes of treated time and 65-70 °C of temperature. The synthesized copper nanoparticles were characterized by optical absorption spectrum, scanning electron microscopy (SEM), and Fourier Transform Infrared Spectrometry.
机译:铜纳米粒子,由于它们的特殊性能,小尺寸和低成本制备,具有许多潜在的应用,例如光学,电子,催化,传感器,抗菌剂。在该研究中,通过具有不同条件的化学还原方法合成铜纳米粒子,以研究给出了发出最小(粒径)尺寸的最佳条件。合成步骤使用铜(II)乙酸盐作为前体,抗坏血酸作为还原剂,甘油和聚乙烯吡咯烷酮(PVP)作为保护剂和稳定剂。超声波的援助被认为是影响合成颗粒尺寸的重要因素。结果表明,铜纳米粒子已成功合成,直径小至20-40nm,超声波的条件为48kHz的频率,处理时间20分钟和65-70℃的温度。通过光学吸收光谱,扫描电子显微镜(SEM)和傅里叶变换红外光谱法以合成的铜纳米颗粒特征。

著录项

相似文献

  • 外文文献
  • 中文文献
  • 专利
获取原文

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号