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Optimization of Pyrrole Electropolymerization on a Steel Gauze Electrode Using the Cyclic Voltammetry Method

机译:循环伏安法测定钢纱布上吡咯电极的优化

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Study on pyrrole electropolymerization is the preliminary step in synthesizing polypyrrole membranes, which can be used for various purposes in biosensor. In this work, electropolymerization process and electrochemical analysis of polypyrrole as an electroactive polymer have been studied by cyclic voltammetry. Pyrrole was electropolymerized to form polypyrrole in an aqueous potassium chloride solution at different pHs using phosphate buffer. The results showed that a potential range of 0-1200 mV is suitable for polypyrrole electropolymerization using the Ag|AgCl electrode as the reference. The formation of polypyrrole is stable at a scan rate of 100 mV/s. In addition, the optimized pyrrole electropolymerization was obtained using 0.1 M pyrrole and phosphate buffer at pH of 2-6. Taken together, this study can be used as a reference for the synthesis of other conducting polymers.
机译:吡咯电聚合的研究是合成聚吡咯膜的初步步骤,其可用于生物传感器中的各种目的。在该工作中,通过循环伏安法研究了作为电活性聚合物的聚吡咯的电聚合过程和电化学分析。使用磷酸盐缓冲液在不同的pH下电解以在不同的pH下在氯化钾水溶液中形成聚吡咯。结果表明,0-1200mV的电位范围适用于使用Ag | AgC1电极作为参考的聚吡咯电极聚合。聚吡咯的形成以100mV / s的扫描速率稳定。此外,使用0.1M吡咯和pH为2-6的磷酸盐缓冲液获得优化的吡咯电聚合。连同,该研究可以用作合成其他导电聚合物的参考。

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