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CHARACTERIZATION OF TI-6AL-4V POWDER IN ELECTRON BEAM MELTING ADDITIVE MANUFACTURING

机译:电子束熔化添加剂制造中Ti-6Al-4V粉末的表征

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In this study, preheated Ti-6V-4V powder from electron beam melting (EBM) additive manufacturing (AM) were experimentally characterized. In the EBM AM process, preheating serves to aggregate the precursor powder, lightly sintered to prevent from the spreading effect. Specimens with sintered Ti-6AL-4V powder enclosed were fabricated and prepared using metallographic means for microstructural and morphology examinations by optical microscopy and scanning electron microscopy. In addition, micro-CT scan was conducted on the specimens and analyzed to study the powder porosity and the powder size distributions. Moreover, the thermal conductivity of preheated powder from EBM AM was measured and analyzed at different temperatures. The results are summarized as follows. Preheating results in metallurgical bonds or even partial melting of the powder. Neck formations are clearly evident in both the Z-plane and Xplane samples. The diameter of the necks is on the order of 1 to 10 μm. In addition, micro-CT analysis shows a similar porosity level between the Z-plane and the X-plane sections. The calculated porosity of the preheated powder is about 50%. Moreover, the major diameter range of the powder is from 30 to 50 μm. The Ti-6Al-4V powder has significantly lower thermal conductivity than that of a solid. The thermal conductivity of Ti-6Al-4V powder is also highly temperature dependent, about 0.63 W/m·K at the room temperature and less than 2.44 W/m·K at 750°C.
机译:在该研究中,通过电子束熔化(EBM)添加剂制造(AM)预热的Ti-6V-4V粉末进行了实验表征。在EBM AM工艺中,预热剂用于聚集前体粉末,轻轻烧结以防止涂抹效果。用光学显微镜和扫描电子显微镜使用金属腔方法制备具有烧结Ti-6AL-4V粉末的标本,并使用金相和形态学检查制备。此外,在试样上进行微型CT扫描,并分析以研究粉末孔隙率和粉末尺寸分布。此外,测量来自EBM AM的预热粉末的导热率并分析在不同的温度下。结果总结如下。预热导致冶金键或甚至是粉末的部分熔化。 Z平面和XPLANE样品中清楚地明显明显。颈部的直径约为1至10μm。另外,微型CT分析在Z平面和X面部分之间示出了类似的孔隙率水平。预热粉末的计算孔隙率为约50%。此外,粉末的主要直径范围为30至50μm。 Ti-6Al-4V粉末的导热率明显低于固体。 Ti-6Al-4V粉末的导热率也是高温依赖性,在室温下约0.63W / m·k,在750℃下小于2.44W / m·k。

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