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Synthesis of Carbon Nanotubes by Chemical Vapour Deposition of Camphor Oil over Ferrocene and Aluminum Isopropoxide Catalyst

机译:樟脑油化学气相沉积合成二茂铁和铝异丙醇氧化盐催化剂的碳纳米管

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The aim of this study is to engage a basic understanding of the information carbon nanotubes (CNTs) may yield when this CNTs is deposited on silicon substrate over ferrocene and aluminum isopropoxide catalyst. Several popular methods are used to produce high quality CNT such as chemical vapour deposition, arc discharge and others. Most promising method is, chemical vapour deposition (CVD), used to produce CNTs in this experiment. The carbon source and catalyst were placed at different alumina boat in furnace one (1). The silicon substrate was placed at the deposition furnace and range temperature from 700°C to 900°C. The G-band peaks of the CNTs appear at round 1580 cm~(-1) and D-band peaks appear at 1348 cm~(-1). Thermal analyses show the percentage of CNTs weight loss 75.12%, 86.39%, 86.54%, 87% and 92.3% respectively. FESEM images was observed to study the formation of the CNTs. The CNTs were successfully synthesized from the chemical vapour deposition method.
机译:该研究的目的是接合对信息碳纳米管(CNT)的基本理解,当该CNT沉积在二茂铁和铝异丙氧化物催化剂上时,该CNT沉积在硅衬底上。 几种流行的方法用于生产高质量的CNT,例如化学气相沉积,电弧放电等。 最有希望的方法是化学气相沉积(CVD),用于在该实验中产生CNT。 将碳源和催化剂置于炉中的不同氧化铝舟皿中(1))。 将硅衬底放置在沉积炉中,范围温度从700℃至900℃。 CNT的G波段峰出现在圆形1580cm〜(-1),D波段峰值出现在1348cm〜(-1)。 热分析显示CNTs重量损失的百分比75.12%,86.39%,86.54%,87%和92.3%。 观察到FESEM图像以研究CNT的形成。 从化学气相沉积方法中成功地合成了CNT。

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