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Characterization of Chemically Synthesized Ag_2Se Nanowires via Anodic Alumina Membrane as Template

机译:通过阳极氧化铝膜作为模板的化学合成Ag_2Se纳米线的表征

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Highly ordered nano crystallized Ag_2Se nanowires of diameter 200 nm have been successfully prepared through direct chemical method using Anodic Alumina Membrane (AAM) as a template; AgNO_3 as cation precursor agent and Na_2SeSO_3 as Se precursor, respectively at room temperature. The qualitative analysis of the EDAX spectrum of nanowires shows that the atomic composition of Ag and Se in synthesized nanowires is close to 2:1 stoichiometry. XRD spectrum confirms orthorhombic structure. UV-Vis absorption spectrum provides estimation of the optical band gap 1.41 eV of nanowires.
机译:通过使用阳极氧化铝膜(AAM)作为模板,通过直接化学方法成功制备了直径200nm的高度有序的纳米结晶Ag_2Se纳米线; AgNO_3分别在室温下作为阳离子前体剂和Na_2SesO_3作为Se前体。纳米线的EDAX光谱的定性分析表明,合成纳米线中的Ag和Se的原子组合物接近2:1个化学计量。 XRD光谱确认正交结构。 UV-Vis吸收光谱提供纳米线的光带隙1.41eV的估计。

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