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Microstructure and Sliding wear Performance of Plasma Sprayed TiB_2-Ni Coatings Deposited from Agglomerate Sintered Powders

机译:沉积来自附聚粉末的等离子体喷涂Tib_2-Ni涂层的微观结构和滑动磨损性能

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This work was aimed at developing a route for the deposition of TiB_2-Ni cermet coating. The feedstock was firstly prepared by agglomerate and sintering, which was subsequently subjected to plasma spraying. The microstructures and the phase composition of the powders, as well as the sprayed coatings were analyzed by SEM and XRD. The micro hardness (Hv) and fracture toughness (K_(IC)) of the coatings were evaluated. Sliding wear tests were also performed on the sprayed coating by SRV tester using GCr15 as a counterpart. The result showed that all the TiB_2-Ni coatings consisted of TiB_2, Ni and Ni_(20)Ti_3B_6 phase, whose amount varied depending on the powder calcination temperature and the TiB_2 content in the powder. Both the hardness and the fracture toughness changed correspondingly. The brittle Ni_(20)Ti_3B_6 phase was the main factor to reduce the fracture toughness of the coatings, which also induced detrimental effect on the slide wear properties. The 60TiB_2-40Ni coating deposited from powder calcined at 1300°C presented better sliding wear performance as it had less amount of Ni_(20)Ti_3B_6 phase and higher amount of TiB_2 was retained in the coating.
机译:这项工作旨在开发沉积TIB_2-NI金属陶瓷涂层的途径。首先通过附聚和烧结制备原料,随后进行等离子体喷涂。通过SEM和XRD分析粉末的微观结构和相组合物以及喷涂涂层。评价涂层的微硬度(HV)和断裂韧性(K_(IC))。通过SRV测试仪使用GCR15作为对应物的SRV测试仪在喷涂涂层上进行滑动磨损试验。结果表明,所有TIB_2-NI涂层由TIB_2,Ni和Ni_(20)TI_3B_6相组成,其量根据粉末煅烧温度和粉末中的TIB_2含量而变化。硬度和断裂韧性相应地发生变化。脆性Ni_(20)Ti_3b_6相是降低涂层断裂韧性的主要因素,这也引起对滑动磨损性能的不利影响。从1300℃煅烧的粉末涂覆的60tib_2-40ni涂层呈现出更好的滑动磨损性能,因为它具有较少量的Ni_(20)Ti_3b_6相,并且保留在涂层中的较高量的Tib_2。

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