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Investigation of the sintering mechanism of steel slag-based ceramics

机译:钢结渣陶瓷烧结机理研究

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In order to manufacture high-value added materials from steel slag, a steel slag-based ceramic was prepared in the paper. X-ray diffraction (XRD) and scanning electron microscopy (SEM) techniques were carried out to characterize the phase formation and the microstructure of the steel slag-based ceramics. Besides, the line shrinkage, flexural strength and water absorption were also determined. Results show that the variation of the line shrinkage and the flexural strength had a positive correlation with the increase of the temperature at the interval 1160°C~1210°C, which was opposite to the change of the water absorption. 1210°C was proved to be the optimum sintering temperature in this work, at which the maximum flexural strength was obtained with a value of 99.39MPa. With the temperature increasing, the quartz phase gradually decreased, participating in the sintering reaction, and the diopside become dominant phase with columnar crystals in 2-5μm at length, which would contribute to the fine performance of the ceramics.
机译:为了制造从钢渣中制造高附加材料,在纸上制备了一种钢制矿物的陶瓷。进行X射线衍射(XRD)和扫描电子显微镜(SEM)技术,以表征钢渣基陶瓷的相形成和微观结构。此外,还确定了线收缩,弯曲强度和吸水性。结果表明,线收缩的变化和弯曲强度与间隔1160°C〜1210℃的温度的增加具有正相关,这与吸水率的变化相反。在该工作中被证明是120℃是最佳烧结温度,获得最大弯曲强度,其值为99.39MPa。随着温度的增加,石英相逐渐降低,参与烧结反应,潜水孔在柱状晶体中以2-5μm的长度变成显性相,这将有助于陶瓷的细化性能。

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