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SAPO-34 zeolites prepared using calcined-MCM-41 as silica source

机译:使用煅烧-MCM-41制备的SAPO-34沸石作为二氧化硅源

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摘要

SAPO-34 molecular sieve was successfully synthesized using calcined-MCM-41 as silica source and morpholine as a template. The influence of MCM-41 content on the synthesis was investigated. The result shows that pure SAPO-34 could be obtained in a wide range of the n (SiO_2)/n (Al_2O_3) ratio in the starting gel. Moreover, increase the n (SiO_2)/n (Al_2O_3) ratio has a negative effect on crystallinity while high silicon incorporates into the framework of SAPO-34.
机译:使用煅烧-MCM-41作为二氧化硅源和吗啉作为模板,成功地合成SAPO-34分子筛。研究了MCM-41含量对合成的影响。结果表明,纯SAPO-34可以在起始凝胶中的宽范围内(SiO_2)/ N(AL_2O_3)比中获得。此外,增加N(SiO_2)/ N(AL_2O_3)比对结晶度的负面影响,而高硅包含在SAPO-34的框架中。

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