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Microstructure Characterization of Large Strain Deformed Fe-32Ni Alloy

机译:大应变变形Fe-32%Ni合金的微观结构表征

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High-resolution electron backscatter diffraction (EBSD) in scanning electron microscope and transmission electron microscope (TEM) were used to investigate the microstructure of Fe-32%Ni alloy processed by large strain multi-axial forging. The samples were compressed with loading direction changed through 90° from pass to pass at temperature of 500°C and a strain rate of 10~(-2)/s. The results show the microstructure evolution is characterized by full development of almost equi-axed fine grains, not well-developed grain boundaries accompanied by high dislocation density and the existence of extensive extinction contours in the vicinity of grain boundaries, and the structure characteristics indicate that the grain boundaries are in a non-equilibrium state with high internal stresses.
机译:扫描电子显微镜和透射电子显微镜(TEM)中的高分辨率电子反向散射衍射(EBSD)用于研究大规模多轴锻造的Fe-32%Ni合金的微观结构。将样品与装载方向压缩,通过通过通过90°改变为500℃的温度和10〜(-2)/ s的应变率。结果表明,微观结构演化的特征在于全面开发几乎等于轴向的细粒,而不是发育良好的晶界,伴随着高位错密度和晶界附近的广泛消光轮廓的存在,并且结构特征表明了这一点晶界处于具有高内应力的非平衡状态。

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