Microwave-Assisted FeCl_3·6H_2O-Catalyzed Regioselective Deprotection of Pyranose Anomeric O-Acetyl Group

机译：微波辅助FECL_3·6H_2O催化的吡喃糖异常O-乙酰基的区域选择性脱保护

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Treatment of peracetylated pyranoses with FeCl_3·6H_2O in acetonitrile under microwave conditions provides an efficient and mild method for regioselective deprotection of anomeric O-acetyl group. The experimental results indicated that the employment of microwave could notably improve the reaction efficacy compared with the conventional heating condition.

机译：在微波条件下，在乙腈中将吡喃酰化吡喃吡喃化物用FECL_3·6H_2O的处理提供了一种有效和温和的方法，用于异常O-乙酰基的区域选择性脱保护方法。实验结果表明，与常规的加热条件相比，微波的就业可以显着提高反应效果。

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《International Conference on Material Engineering, Chemistry, Bioinformatics》|2014年||共4页
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Qiang Wang; Guodong Liu; Shanshan Gong; Qi Sun;
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中图分类 TB3-53;
关键词
Pyranose; Regioselective deacetylation; Deprotection; Microwave; FeCl_3·6H_2O;

机译：吡喃糖;区域选择性脱乙酰化;去脱离;微波;fecl_3·6h_2o;

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1. Regioselective deprotection of the monosaccharide-bearing thiocyanomethyl group at the anomeric position monitored by reversed-phase HPLC method [J] . Abualassal Qais, Al Azzam Khaldun M., Jilani Jamal A. Biomedical Chromatography: An International Journal Devoted to Research in Chromatographic Methodologies and Their Applications in the Biosciences . 2016,第9期

机译：反相HPLC法监测端基上带有单糖的硫氰基甲基的区域选择性脱保护
2. Facile synthesis of nonsymmetrical heteroaryl-substituted triarylmethanes via the FeCl_3•6H_2O-catalyzed two-step Friedel-Crafts-type reaction [J] . S. Ruengsangtongkul, P. Taprasert, U. Sirion, Organic & biomolecular chemistry . 2016,第36期

机译：FeCl_3•6H_2O催化的两步Friedel-Crafts型反应易于合成不对称杂芳基取代的三芳基甲烷
3. Anomeric effect in pyranose-ring derivatives containing carbon, silicon, and germanium as anomeric centers: an ab initio systematic study [J] . Rodriguez Ortega P. G., Montejo M., Sanchez Valera M., Structural Chemistry . 2019,第6期

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4. Microwave-Assisted FeCl_3·6H_2O-Catalyzed Regioselective Deprotection of Pyranose Anomeric O-Acetyl Group [C] . Qiang Wang, Guodong Liu, Shanshan Gong, International Conference on Material Engineering, Chemistry, Bioinformatics . 2014

机译：微波辅助FECL_3·6H_2O催化的吡喃糖异常O-乙酰基的区域选择性脱保护
5. The dependence of pyranose ring puckering on anomeric configuration: methyl idopyranosides [O] . Benedict M. Sattelle, Bidisha Bose-Basu, Matthew Tessier, -1

机译：吡喃糖环PACKERION在异常配置中的依赖性：甲基骨甲醛
6. Dependence of pyranose ring puckering on anomeric configuration: Methyl idopyranosides [O] . Sattelle, Benedict M., Bose-Basu, Bidisha, Tessier, Matthew, 2012

机译：吡喃环起球对异头构型的依赖性：甲基idopyranosides

Microwave-Assisted FeCl_3·6H_2O-Catalyzed Regioselective Deprotection of Pyranose Anomeric O-Acetyl Group

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