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Preparation and Applications of Precious Metals Adsorbed Activated Carbon Cloth

机译:贵金属吸附活性炭布的制备及应用

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Precious metal nanoparticles (e.g. Au, Pd and Pt) on activated carbon cloths (ACCs) were simply prepared by impregnation of metal salts dissolving in ethanol solution. Pretreatment of the ACCs was firstly performed in hydrochloric acid solution and nitric acid as oxidizing agent was employed in order to introduce oxygen complex on the ACCs fiber surfaces. Uniformly dispersed metal nanoparticles with diameter of 5-20 nm on the ACC surfaces were simply achieved without using reducing agents. Morphology and composition of the metal adsorbed ACCs were examined by Scanning Electron Microscopy (SEM) and Energy Dispersive Spectroscopy (EDS), respectively. Electrolytic activity of metal/ACCs was investigated by using cyclic voltammetry (CV) to demonstrate the electron-transfer properties. Results demonstrate that metals adsorbed ACCs were easily prepared with simple procedures which will be more convenient for preparations and applications.
机译:通过浸渍溶解在乙醇溶液中的金属盐制备的贵金属纳米颗粒(例如,Au,Pd和Pt)。首先在盐酸溶液中进行预处理,采用硝酸作为氧化剂,以在ACCs纤维表面上引入氧气。在不使用还原剂的情况下,简单地实现了Acc表面上直径为5-20nm的均匀分散的金属纳米颗粒。通过扫描电子显微镜(SEM)和能量分散光谱(EDS)来检查金属吸附ACC的形态和组成。通过使用循环伏安法(CV)来研究金属/ ACC的电解活性,以证明电子转移性能。结果表明,通过简单的程序易于制备金属吸附ACC,这对于制剂和应用更方便。

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