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Microstructural Evolution of Tungsten/Zirconium Hafnium Carbides Composites During Consolidation Processes

机译:固结过程中钨/锆碳化物复合材料的微观结构演化

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The paper describes the fabrication process of refractory carbides, ZrC and HfC, dispersed tungsten composites by spark plasma sintering. The contents of particles varied from 0 to 30 vol % and sintering was conducted for 3 min at 1700°C. After the sintering of W/ZrC powder mixtures, ZrC phases were decomposed into W_2C and Zr up to 20 vol% of ZrC particles. With 30 vol% of particles, some of ZrC particles were retained in the composite. However, although the amount of HfC particles was increased, most of HfC phases were remained. From these results, HfC particles seemed to be more stable phase in the tungsten matrix at high temperature.
机译:本文描述了耐火碳化物,ZRC和HFC的制造过程,通过火花等离子体烧结分散钨复合材料。颗粒的含量在0至30体积%中变化,在1700℃下对3分钟进行烧结。在烧结W / ZRC粉末混合物之后,ZrC相分解成W_2C和Zr至20体积%的ZrC颗粒。含有30体积粒的颗粒,将一些Zrc颗粒保留在复合材料中。然而,尽管HFC颗粒的量增加,但仍保持大多数HFC相。从这些结果中,HFC颗粒在高温下钨基质中的相位似乎更稳定。

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