The 4.5mm wide 25μm thick Fe_(78)Si_9B_(13) amorphous alloys were prepared by single-roller method, and it was annealed. The elastic modulus, tensile deformation and line expansion coefficient were investigated by Q800 (dynamic mechanical thermal analyses, DMA). The results showed that the elastic modulus, tensile deformation and line expansion coefficient were enhanced when annealed. Comparing with the annealed ribbons, the change rules of elastic modulus, tensile deformation and line expansion coefficient of the quenched are evident, that the elastic modulus decreases and tensile deformation increase with temperature increases, but line expansion coefficient firstly increase then decrease with temperature increases.
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