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Comparison of CVD and MOCVD-grown Al2O3 coatings in the performance of cemented carbide cutting tool inserts

机译:CVD和MOCVD-生长的Al2O3涂层在碳化物切削工具插入物性能下的比较

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Low-pressure MOCVD, with tris(2,4-pentanedionato)aluminum(III) as the precursor, was used in the present investigation to coat alumina on to cemented carbide cutting tools. To evaluate the MOCVD process, the efficiency in cutting operations of MOCVD-coated tools was compared with that of tools coated using the industry-standard CVD process. Three multilayer cemented carbide cutting tool inserts, viz., TiN/TiC/WC, CVD-coated Al2O3 on TiN/TiCAVC, and MOCVD-coated Al2O3 on TiN/TiC/WC, were compared in the dry turning of mild steel. Turning tests were conducted for cutting speeds ranging from 14 to 47 m/min, for a depth of cut from 0.25 to 1 mm, at the constant feed rate of 0.2 mm/min. The axial, tangential, and radial forces were measured using a lathe tool dynamometer for different cutting parameters, and the machined work pieces were tested for surface roughness. The results indicate that, in most of the cases examined, the MOCVD-coated inserts produced a smoother surface finish, while requiring lower cutting forces, indicating that MOCVD produces the best-performing insert, followed by the CVD-coated one. The superior performance of MOCVD-alumina is attributed to the co-deposition of carbon with the oxide, due to the very nature of the precursor used, leading to enhanced mechanical properties for cutting applications in harsh environment.
机译:低压MOCVD,与三(2,4-戊二酮)铝(III)作为前体,在本调查涂覆氧化铝上至硬质合金切削刀具使用。为了评估MOCVD工艺,在切割的MOCVD涂层刀具行动的效率与使用业界标准的CVD工艺涂层刀具相比。三个多层硬质合金切削刀具刀片,即,锡/的TiC / WC,CVD涂覆的氧化铝上的TiN / TiCAVC,和MOCVD涂覆Al2O3对锡/的TiC / WC,在干车削低碳钢的进行了比较。车削试验用于切割速度范围为14至47米/分,用于切割从0.25的深度为1毫米,以0.2毫米/分钟的恒定进料速率进行。轴向,切向和径向力分别使用车床工具测力计为不同的切削参数测量,并且所加工的工件中测试了表面粗糙度。结果表明,在大多数情况下检查,所述MOCVD涂层刀片产生更平滑的表面光洁度,同时要求降低切削力,表明MOCVD产生最佳执行插入,随后通过CVD涂覆的一个。 MOCVD氧化铝的优异性能归因于与氧化物,碳的共沉积,由于使用的前体的性质,从而导致恶劣环境下的切割应用增强的机械性能。

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