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Effect of Heat Treatment on the Microstructures and Mechanical Properties in AZ31 Magnesium Alloy Processed by Continuous Rheo-Extrusion

机译:热处理对连续Rheo挤出处理AZ31镁合金微观结构和机械性能的影响

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AZ31 magnesium alloy profiles were prepared by continuous rheo-extrusion process, and effects of solution and aging treatments on the microstructures and mechanical properties was investigated by OLYMPUS optical microscope, scanning electron microscope, energy dispersive spectroscopy device and tensile machine. The results reveal that saturated solid solution was formed in the profile at a solution temperature of 415°C and 16 hours. During aging treatment of saturated solid solution, β-Mg_(17)Al_(12) phase nucleates firstly at grain boundaries and takes on globular growth, which is mainly due to the lower interfacial energy in coherent or semi-coherent interface between β-Mg_(17)Al_(12) phase and matrix phase. Lower interfacial energy is favorable to the nucleation and growth of β-Mg_(17)Al_(12) phase at grain boundary. With the increase of aging time or the rise of aging temperature, β-Mg_(17)Al_(12) phase precipitates out gradually from grain interior and starts to grow in globular shape. After β-Mg_(17)Al_(12) phase grows to a certain extent, it grows in lamellar shape along the orientation of lower mismatch between β-Mg_(17)Al_(12) phase and matrix phase. After solution at 415°C and 16h and aging at 180°C and 8h, the ultimate tensile strength and elongation to failure of the profile are 305MPa and 13%, respectively.
机译:通过连续的Rheo挤出方法制备AZ31镁合金型材,并通过奥林巴斯光学显微镜,扫描电子显微镜,能量分散光谱装置和拉伸机研究了溶液和老化处理对微观结构和机械性能的影响。结果表明,在415℃和16小时的溶液温度下形成饱和固溶体。在饱和固溶溶液的老化处理期间,β-Mg_(17)Al_(12)相位首先在晶界中成核,并具有球状生长,这主要是由于β-Mg_之间相干或半相干界面中的界面能量较低或较低的界面能量。 (17)AL_(12)相和矩阵阶段。较低的界面能量有利于晶界β-Mg_(17)Al_(12)相的成核和生长。随着老化时间的增加或衰老温度的升高,β-Mg_(17)Al_(12)相逐渐从谷物内部逐渐沉淀,开始以球状形状生长。在β-Mg_(17)Al_(12)相之后在一定程度上生长,它沿着β-Mg_(17)Al_(12)相和基质相之间的较低失配的取向成了层状形状。在415℃和16小时溶液后,在180℃和8h时老化,曲线的最终拉伸强度和曲线衰竭的伸长率分别为305MPa和13%。

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