Electrospinning has gained substantial attention in both academic and industrial research as an efficient approach to producing continuous fibers with diameter ranging from tens of nanometers to several micrometers [1]. In recent years, with the rapid progress in the synthesis process of electrospinning technique, the scope of its applications has been broadened to the fields of optoelectronics, catalyst, filtration and medicine, while the investigation of the electrospun materials as electrochemical sensors is still in its infancy. Recently, we prepared the novel electrospun carbon materials and explored their good electroanalytical properties as amperometric sensors [2-5]. Herein, further investigation was conducted by designing nonenzymatic glucose sensor with novel electrospun nanocomposite.
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