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A Study on the Influence of Surface Active Agent Molecules on the AFM Scanning and Imaging of SWCNTs

机译:表面活性剂分子对SWCNTS的AFM扫描和成像的影响研究

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The paper proposed a preprocessing method for scanning samples based on rinsing technology, and solved the effective fabrication problem of AFM scanning samples based on facilitated dispersing sWCNTs with SDS surface active agents. First, the ultrasonication oscillation method was applied, and the uniform alignment of SWCNTs in SDS was realized. Then, SDS solution of different concentrations was scanned and imaged with AFM, the influence of SDS solution on the imaging quality of SWCNTs was analyzed, and the method to effectively fabricate scanning samples after dispersing SWCNTs was found. The results of the experiments showed that the preprocessing of the SWCNTs solution scanning samples was the decisive factor to influence SWCNTs imaging quality, that the result of rinsing SWCNTs scanning samples for 5s at 0.1ml/s with di-ionized water was the best, and that with the same rinsing rate and angle, the rinsing di-ionized water quantity would influence the alignment degree of SWCNTs on the substrates and SDS macromolecules' residual quantity on SWCNTs scanning samples.
机译:本文提出了一种基于漂洗技术扫描样品的预处理方法,并基于促进分散的SWCNTS解决了AFM扫描样品的有效制造问题,其具有SDS表面活性剂。首先,施加超声波振荡方法,实现了SWCNTS在SDS中的均匀取向。然后,用AFM扫描和成像不同浓度的SDS溶液,分析了SDS溶液对SWCNT的成像质量的影响,并发现了在分散SWCNTS之后有效制造扫描样品的方法。实验结果表明,SWCNTS溶液扫描样品的预处理是影响SWCNT成像质量的决定性因素,即漂洗SWCNTS扫描样品的5S在0.1ml / s的下离子水的结果是最好的,并且具有相同的漂洗速率和角度,漂洗二离子水量将影响基质上的SWCNT的对准度和SDS大分子在SWCNTS扫描样品上的残余量。

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