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Parametric Studies of Thin Film Nickel Catalyst for the Growth of Carbon Nanotubes

机译:薄膜镍催化剂的参数研究碳纳米管生长

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The thickness and morphology of the catalyst film significantly affect the properties of carbon nanotubes (CNTs). The catalyst size and shape are the key factors for the controlling of CNT diameter. Therefore, the objectives of this study are to develop a thin catalyst film for CNTs growth application by varying the time of deposition and investigate the effect of radio frequency (rf) plasma power. The thin catalyst film was developed using physical sputtering method with an rf power between 20 to 100 watt at varying deposition time with nickel as a catalyst. The Ni/Cr film in this study was fabricated on corning glass substrates. The thin film nickel catalyst was obtained with a thickness of 12 nm using surface profiler and was characterized using field emission scanning electron microscopy (FESEM) and atomic force microscopy (AFM) to determine the morphologies and particle size of the catalyst. It was observed that structural morphology of thin Ni film is influenced by rf power and deposition time.
机译:催化剂膜的厚度和形态显着影响碳纳米管(CNT)的性质。催化剂尺寸和形状是控制CNT直径的关键因素。因此,该研究的目的是通过改变沉积时间来开发用于CNTS生长施加的薄催化剂膜,并研究射频(RF)等离子体功率的影响。使用物理溅射方法开发薄催化剂膜,其具有在20至100瓦特之间的RF功率,以与镍作为催化剂的不同沉积时间。本研究中的Ni / Cr膜在康宁玻璃基板上制造。使用表面分析仪厚度为12nm获得薄膜镍催化剂,并使用现场发射扫描电子显微镜(FeSEM)和原子力显微镜(AFM)的表征以确定催化剂的形态和粒度。观察到薄Ni膜的结构形态受Rf功率和沉积时间的影响。

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