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Thermal Exposure Effects on Mechanical Behavior of Iron-Based Metallic Glass

机译:热曝光对铁基金属玻璃力学行为的影响

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Hot Micro-hardness testing of drop cast ingots of fully amorphous SAM 1651 (Fe48Mo14Cr_(15)Y_2C_(15)B_6) produced by Oak Ridge National Laboratory was performed in order to determine the behavior of this Fe- bulk metallic glass under a variety of different test conditions. The effects of changes in test temperature on the micro-hardness/strength were determined over the temperature range from room temperature to 620 deg C. Although high (e.g. > 12 GPa) microhardness was exhibited at room temperature, significant hardness reductions were exhibited near Tg. Identical tests were conducted on Alloy C-22 and AISI 316L Stainless Steel for comparison and revealed much lower micro-hardness/strength at room temperature but relatively small changes in micro-hardness from room temperature to 620 deg C. In addition, the effect of exposure time at elevated temperature on the evolution of micro-hardness/strength was also evaluated for selected temperatures between 25 deg C and 620 deg C. Longer term thermal exposures at 150 deg C and 275 deg C were also conducted, followed by x-ray diffraction in order to determine the effects of low temperature long-term thermal exposures on the evolution of any structure. Exposures up to 102 days at 150 deg C and 55 days at 275 deg C did not reveal any changes in XRD, indicating stability of the structure at least up to the number of days exposed to this point.
机译:通过橡树岭国家实验室生产的全无定形SAM 1651(FE48MO14CR_(15)Y_2C_(15)Y_2C_(15)B_6)的热微硬度试验,以确定此FE-散装金属玻璃的行为不同的测试条件。在室温至620℃的温度范围内测定测试温度变化对微硬度/强度的影响。尽管在室温下表现出高(例如> 12GPa)显微硬度,但在TG附近表现出显着的硬度降低。在合金C-22和AISI 316L不锈钢上进行相同的测试,用于比较,并在室温下显露得多微硬度/强度,但是从室温到620℃的微硬度变化相对较小。此外,还有在升高温度下对微硬度/强度的进化的曝光时间也在25℃和620℃之间的选定温度评价在150℃和275℃下的长期热曝光,然后进行X射线衍射以确定低温长期热曝光对任何结构的演变的影响。暴露在150℃和55天的暴露于275℃,275℃下的55天没有揭示XRD的任何变化,表明结构的稳定性至少达到此时暴露的天数。

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