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Impact of Additional gamma' Strengthening on the Strength and Fatigue Behavior of Oxide Dispersion Strengthened Ni-Base Superalloys

机译:额外γ'加强对氧化物分散体强化和疲劳行为的影响强化Ni碱基超合金

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The impact of additional gamma' precipitation hardening on the strength and fatigue life of oxide dispersion strengthened nickel-base superalloys is investigated using the novel alloy, PM 3030. A typical coarse and elongated grain structure is used to compare PM 3030 with a solely oxide dispersion strengthened superalloy PM 1000 having similar chemical composition and grain structure [1]. Constant extension rate tests (CERT) and high cycle fatigue (HCF) tests are performed in the temperature range between room temperature and 1250 deg C in order to evaluate the material performance. Furthermore, optical microscopy, scanning and transmission electron microscopy (SEM and TEM) are performed for the characterization of the microstructure prior to and following mechanical testing. It is found that additional gamma' strengthening in PM 3030 results in an increase in quasi-static strength by about factor 2 and in HCF life at a given stress amplitude by more than factor 4 at temperatures up to 850 deg C as compared to PM 1000. This advantage decreases at temperatures above 850 deg C due to accelerated creep processes, circumvention of gamma' particles, as well as microstructural softening by dissolution of gamma' precipitates [2-3]. When the fatigue behaviour is compared at a fixed ratio of stress amplitude to ultimate compression strength ratio, PM 3030 shows a shorter life time compared to PM 1000 indicating that the gain in quasi-static strength is greater than that in fatigue strength. It can be concluded that combining oxide dispersion and precipitation strengthening has a great potential for intermediate temperature applications, i.e. at service temperatures between 600 and 1160 deg C.
机译:使用新的合金,PM 3030研究了额外的γ'沉淀硬化对氧化物分散的强度和疲劳寿命的影响。典型的粗糙和细长的晶粒结构用于将PM 3030与单独的氧化物分散体进行比较加强超合金PM 1000具有相似的化学成分和晶粒结构[1]。在室温和1250℃之间的温度范围内进行恒定扩展速率测试(CERT)和高循环疲劳(HCF)测试,以评估材料性能。此外,对机械测试之前和之后的微结构表征进行光学显微镜,扫描和透射电子显微镜(SEM和TEM)。发现PM 3030的额外γ'加强强化导致准静态强度在给定的应力幅度在给定的应力幅度下增加超过850℃,与PM 1000相比,在给定的应力幅度下的因子2中增加。 。由于加速蠕变过程,通过溶解γ'沉淀物的溶解[2-3],这种优势在850℃以上的温度下降到850℃以上850℃的温度下降,以及通过溶解的微观组织软化[2-3]。当以压力幅度与极限压缩强度比的固定比率比较疲劳行为时,PM 3030显示与PM 1000相比的寿命较短,表明准静态强度的增益大于疲劳强度的增益。可以得出结论,组合氧化物分散和沉淀强化具有巨大的中间温度应用的潜力,即在600至1160℃之间的服务温度。

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