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Behavior of Quartz and Carbon Black Pellets at Elevated Temperatures

机译:升高温度下石英和炭黑颗粒的行为

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This paper studies the quartz and carbon black pellets at elevated temperature with varying temperature and gas atmosphere. High-purity quartz and commercial ultra-pure carbon black was mixed (carbon content tvt.15%), and then pelletized into particles of l-3mm in diameter. The stoichiometric analysis of the pellet during heating is studied in thermogravimetric analysis (TGA) furnace at different temperature in CO and Ar atmosphere. The microstructure, phase changes and element content of sample before/after heating is characterized by X-ray diffraction, scanning electron microscope, X-ray fluorescence and LECO analyzer. The reaction process can be divided into two stages. Higher temperature and argon atmosphere are the positive parameters for SiC formation.
机译:本文研究了升高温度下的石英和炭黑颗粒,温度和气体气氛。高纯度石英和商业超纯炭黑混合(碳含量TVT.15%),然后将直径L-3mm的颗粒造成颗粒。在CO和AR气氛中的不同温度下的热重分析(TGA)炉中研究了加热过程中颗粒的化学计量分析。在加热之前/后样品的微观结构,相变和元素含量的特征在于X射线衍射,扫描电子显微镜,X射线荧光和LECO分析仪。反应过程可分为两个阶段。较高的温度和氩气氛是SiC形成的阳性参数。

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