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Effect of Surface Oxide Layer on Mechanical Properties of Single Crystalline Silicon

机译:表面氧化物层对单晶硅机械性能的影响

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This paper reports on the tensile testing of single crystal silicon (SCS), whose specimen surface was intentionally oxidized, and the effect of the oxide thickness on the mechanical properties in order to investigate the fatigue fracture mechanism under cyclic loading. SCS specimens were fabricated from silicon-on-insulator (SOI) wafer with 3-μm -thick device layer and oxide layer were grown to the specimens using thermal dry oxidation at 1100 °C. The specimen test part was 120 or 600 μm long and 4 μm wide. Quasi-static tensile testing of SCS specimen without oxide layer, with 100-nm-thick oxide, and with 200-nm-thick oxide was performed. As the results, the fracture origin location changed from the surface of the specimen of SCS without oxide to inside of silicon of oxidized specimen. This change may be caused by the smoothing of the surface and formation of oxide precipitation defects in silicon during oxidation. The estimated radius of the defects in specimen with 100 -nm-thick oxide and with 200-nm-thick oxide was 26 nm and 45 nm, respectively, which is well agreed with the fracture-initiating crack sizes calculated from the measured strengths.
机译:本文报道了单晶硅(SCS)的拉伸试验,其样本表面有意氧化,氧化物厚度对机械性能的影响,以研究循环载荷下的疲劳断裂机制。 SCS样本由绝缘体(SOI)晶片制成,使用3μm-Thick装置层,并在1100℃下使用热干氧化生长到试样的氧化物层。样品试验部分为120或600μm长,4μm宽。进行氧化物层的SCS样品的准静态拉伸试验,具有100nm厚的氧化物,含有200nm厚的氧化物。作为结果,裂缝起源位置从SCS样品的表面改变而没有氧化物到氧化标本的硅内部。这种变化可能是由氧化过程中硅表面的平滑和氧化物沉淀缺陷的平滑引起的。具有100℃厚的氧化物和200nm厚的氧化物的样品中缺陷的估计半径分别为26nm和45nm,这与由测量的强度计算的裂缝引发裂纹尺寸很好。

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