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The seeding effect of lanthanum nickel oxide ceramic/ceramic nanocomposite thin films prepared by the MOD method

机译:镧氧化镍氧化镍陶瓷/陶瓷纳米复合薄膜的播种作用Mod法制备

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Lanthanum nickel oxide (LNO) is a conducting ceramic which has potential to be used as electrodes in multilayer ceramic actuators. Thick LNO films have been formed by incorporating nanosized LNO powder (annealed at 700°C, with diameter around 100 nm) into a LNO solution prepared by a metal-organic decomposed ( MOD ) method. Three different weight percents, 2%, 4%, and 10% of LNO powder have been added. The structural variation of the ceramic/ceramic composite film with annealing temperature was studied by X-ray diffraction and differential thermal analysis. The crystallization temperature of the film is found to decrease from ~590°C to ~510°C due to the seeding effect introduced by the nano-powder.
机译:镧镍氧化镍(LNO)是导电陶瓷,其具有多层陶瓷致动器中的电极用作电极。通过将纳米化的LNO粉末(以700℃,直径约为100nm退火)加入通过金属 - 有机分解(MOD)方法制备的LNO溶液来形成厚的LNO膜。已经添加了三种不同的体积,2%,4%和10%的LNO粉末。通过X射线衍射和差分热分析研究了与退火温度的陶瓷/陶瓷复合膜的结构变化。由于纳米粉末引入的播种效果,发现薄膜的结晶温度从〜590℃降至约510℃。

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