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Study of Low-Grade Nickel Laterite Processing Using Palm Shell Charcoal as Reductant

机译:棕榈壳炭还原低品位红土镍矿的研究

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This study was conducted to investigate the effect of palm shell charcoal reductant in the selective reduction of nickel ore with the addition of additive at various temperatures and times. In this present work, 10 wt. % of sodium sulfate as additive and 5, 10, 15 wt. % of palm shell charcoal as reductants were used. The reduction of nickel ore was performed at 950°C, 1050°C, and 1150°C for 60, 90, and 120 minutes. A wet magnetic separation method was then carried out to separate the concentrates and tailings. Characterization of reduced ore was performed by X-Ray Diffraction (XRD) and Scanning Electron Microscope (SEM) with Energy Dispersive X-ray Spectroscopy (EDS), while the composition of ferronickel in concentrate was identified by X-Ray Fluorescence (XRF). The result showed that the higher temperature reduction, the higher of nickel grade, and its recovery at the concentrate. Nevertheless, the longer reduction time and the more reductant in nickel ore lowering the nickel grade and its recovery in the concentrate. The optimum condition in this selective reduction process was obtained with the addition of 5 wt. % of reductant and 10 wt. % of sodium sulfate in nickel ore, which was reduced at 1150°C for 60 minutes. It resulted in 4.60% and 73.23% for nickel grade and its recovery, respectively.
机译:本研究旨在研究棕榈壳炭还原剂在不同温度和时间下添加添加剂选择性还原镍矿石的效果。在本研究中,使用10 wt.%的硫酸钠作为添加剂,5,10,15 wt.%的棕榈壳木炭作为还原剂。镍矿石的还原在950℃、1050℃和1150℃下进行60、90和120分钟。然后采用湿式磁选法分离精矿和尾矿。通过X射线衍射(XRD)和扫描电子显微镜(SEM)以及能量色散X射线光谱(EDS)对还原矿石进行表征,同时通过X射线荧光(XRF)对精矿中的镍铁成分进行鉴定。结果表明,还原温度越高,镍品位越高,精矿中镍的回收率也越高。然而,还原时间越长,镍矿中还原剂越多,镍品位和精矿中镍的回收率就会降低。通过在镍矿中添加5%(重量百分比)的还原剂和10%(重量百分比)的硫酸钠,在1150°C下还原60分钟,获得了该选择性还原过程的最佳条件。镍品位和回收率分别为4.60%和73.23%。

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