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Helium Mass Spectrometer Leak Detection: A Method to Quantify Total Measurement Uncertainty

机译:氦质谱仪泄漏检测:一种量化总测量不确定性的方法

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In applications where leak rates of components or systems are evaluated against a leak rate requirement, the uncertainty of the measured leak rate must be included in the reported result. However, in the helium mass spectrometer leak detection method, the sensitivity, or resolution, of the instrument is often the only component of the total measurement uncertainty noted when reporting results. To address this shortfall, a measurement uncertainty analysis method was developed that includes the leak detector unit's resolution, repeatability, hysteresis, and drift, along with the uncertainty associated with the calibration standard. In a step-wise process, the method identifies the bias and precision components of the calibration standard, the measurement correction factor (K-factor), and the leak detector unit. Together these individual contributions to error are combined and the total measurement uncertainty is determined using the root-sum-square method. It was found that the precision component contributed more to the total uncertainty than the bias component, but the bias component was not insignificant. For helium mass spectrometer leak rate tests where unit sensitivity alone is not enough, a thorough evaluation of the measurement uncertainty such as the one presented herein should be performed and reported along with the leak rate value.
机译:在评估泄漏率要求的组分或系统的泄漏速率的应用中,必须将测量的泄漏率的不确定性包含在报告的结果中。然而,在氦质谱仪泄漏检测方法中,仪器的灵敏度或分辨率通常是报告结果时唯一注意到的总测量不确定性的组成部分。为了解决这一短缺,开发了一种测量不确定性分析方法,其包括泄漏检测器单元的分辨率,可重复性,滞后和漂移以及与校准标准相关的不确定性。在逐步过程中,该方法识别校准标准,测量校正因子(K系列)和泄漏检测器单元的偏置和精确组件。将这些个体对误差的贡献组合在一起,并且使用根和方形方法确定总测量不确定性。发现精密组分贡献比偏置分量更多的不确定度,但偏置分量并不微不足道。对于氦质谱仪泄漏率测试,其中单独的单位灵敏度是不够的,应当对诸如本文所呈现的一个诸如本文所呈现的测量不确定性的彻底评估和报告。

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