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EFFECTS OF TEMPERATURE AND STEAM ENVIRONMENT ON CREEP BEHAVIOR OF AN OXIDE-OXIDE CERAMIC COMPOSITE

机译:温度与蒸汽环境对氧化氧化物陶瓷复合材料蠕变行为的影响

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The tensile creep behavior of an oxide-oxide continuous fiber ceramic composite (CFCC) was investigated at 1000 and 1100 deg C in laboratory air and in steam. The composite consists of a porous alumina matrix reinforced with laminated, woven mullite/alumina (Nextel~(TM)720) fibers, has no interface between the fiber and matrix, and relies on the porous matrix for flaw tolerance. The tensile stress-strain behavior was investigated and the tensile properties measured. Tensile creep behavior was examined for creep stresses in the 80-150 MPa range. Primary and secondary creep regimes were observed in creep tests at all temperatures investigated. Creep rates increased with increasing temperature and creep stress. The presence of steam accelerated creep rates and dramatically reduced creep life. The detrimental effects of steam become progressively more pronounced with increasing temperature. At 1000 deg C, creep run-out defined as 100 h at creep stress was achieved in all tests. At 1100 deg C, creep run-out was achieved in all tests in air and only in the 100 MPa test in steam. The residual strength and modulus of all specimens that achieved run-out were characterized. Composite microstructure, as well as damage and failure mechanisms were investigated.
机译:在实验室空气和蒸汽中,在1000和1100℃下研究氧化氧化物连续纤维陶瓷复合物(CFCC)的拉伸蠕变行为。复合材料由具有层压的纺织莫来石/氧化铝(Nextel〜(TM)720)纤维增强的多孔氧化铝基质组成,在纤维和基质之间没有界面,并且依赖于多孔基质进行缺陷耐受性。研究了拉伸应力 - 应变行为,测定拉伸性能。在80-150MPa范围内检查拉伸蠕变行为。在研究的所有温度下,在蠕变试验中观察到初级和二次蠕变制度。随着温度和蠕变压力的增加而增加,蠕变率会增加。蒸汽加速蠕变速率的存在并显着降低了蠕变寿命。随着温度的增加,蒸汽的不利影响变得逐渐变得更加明显。在所有测试中,在1000℃下,在蠕变应力下定义为100h的蠕变耗尽。在1100℃下,在空气中的所有测试中实现了蠕变耗尽,并且仅在蒸汽中的100MPa测试中获得。表征了达到射流的所有样品的残余强度和模量。研究了复合微观结构,以及损坏和破坏机制。

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