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Indentation crack healing in low glass-content mullite

机译:低玻璃含量莫来石缩进裂纹愈合

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The healing of cracks during the heat treatment of mullite ceramics has been studied. Bending bars with indentations were kept at 1300°C for 2 hrs. The length of the indentation cracks before and after the heat treatment were measured and character of the crack healing was studied using scanning electron microscopy in order to identify the healing micromechanisms. The heat-treated bars were broken in four-point bending at room temperature and the resulting flexure strength was compared to that of the indented bars without heat treatment. Extensive reduction of the crack lengths of about 20-35% was found and the indentation flexural strength increased accordingly. The healing took place due to wetting of the crack by glassy phase. The fracture toughness increased because of the crack tip blunting and forming of the glass bridges between the crack faces. It was found that a small pre-loading during the heat treatment which was to prevent the crack closure reduced the extent of the crack healing but did not affect the resulting flexural strength.
机译:研究了在莫来石陶瓷热处理期间裂缝的愈合。用压痕弯曲杆在1300℃下保持2小时。测量热处理前后的压痕裂缝的长度,使用扫描电子显微镜研究了裂纹愈合的特征,以识别愈合微机制。在室温下在四点弯曲中断开热处理的棒,并将得到的弯曲强度与凹槽的没有热处理。发现大约20-35%的裂缝长度的广泛降低,压痕弯曲强度相应增加。通过玻璃相润湿裂缝,愈合发生。由于裂纹尖端的裂纹尖端钻孔和在裂纹面之间形成玻璃桥而增加,断裂韧性增加。结果发现,在热处理期间的小预载荷是为了防止裂纹闭合降低裂纹愈合的程度,但不影响所产生的弯曲强度。

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