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MODIFICATION OF WOOL FIBER BY STEAM EXPLOSION

机译:蒸汽爆炸改变羊毛纤维

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Wool fiber was modified by steam explosion at different pressure in the experiment reported in this paper. After the modification of the steam explosion, SEM results show that some scales on the wool fiber were destroyed and some tiny grooves were produced on the surface of the fiber. FTIR tested results show that there were no evident changes in the chemical composition of the fiber during the explosion treatment. X-Ray tested results show that the crystallinity of the fiber decreased as the treating pressure increased, which agrees well with the thermal analysis results. In the thermal analysis, results of DSC show that the temperatures respectively corresponding to vaporization of water and cleavage of S-S-bond decreased as the explosion pressure increased. The decrease of the thermal decomposition energy of the treated fiber indicates that steam explosion perhaps destroyed some crystals arid some crosslinks of macromolecular chains in the fiber. The treatment also leads to some changes of the fiber properties, including the decrease of the moisture regain and slightly decrease of the solubility in caustic solution.
机译:本文报道的实验中的不同压力下的蒸汽爆炸改性了羊毛纤维。在改变蒸汽爆炸后,SEM结果表明,羊毛纤维上的一些鳞片被破坏,在纤维表面上产生一些微小的凹槽。 FTIR测试结果表明,爆炸处理过程中纤维的化学成分没有明显的变化。 X射线测试结果表明,随着治疗压力的增加,纤维的结晶度降低,这与热分析结果吻合良好。在热分析中,DSC的结果表明,随着爆炸压力的增加,分别对应于水蒸发和S-S键的切割的温度降低。经处理的纤维的热分解能量的降低表明蒸汽爆炸可能破坏了一些晶体在纤维中产生了一些大分子链的交联。该处理还导致纤维性能的一些变化,包括湿度降低,并在苛性溶胶溶液中溶解度略微降低。

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