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APT/SANS characterization of nanometer Cu precipitates in irradiated model alloys

机译:纳米Cu沉淀在辐照模型合金中的Apt / Sans

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The influence of manganese additions on the initial stages of the formation of copper-enriched precipitates has been investigated in Fe-0.8 at.% Cu (VH) and Fe-0.78 at.% Cu-1.05% Mn (VD) model alloys that were neutron irradiated to low fluences. These experiments are a continuation of previous atom probe tomograph (APT) and small angle neutron scattering (SANS) characterizations of these model alloys. In the previous study, these alloys were neutron irradiated to fluences of 1 * 10~(23) n m~(-2) (E > 1 MeV) [1]. In these new experiments, the VH and VD alloys were neutron irradiated to lower fluences of 4 * 10~(21) n m~(-2) and 5 * 10~(22) n m~(-2) at a temperature of 288 °C. The specimens that were neutron irradiated to a fluence of 5 * 10~(22) n m~(-2) were also examined after a post irradiation anneal (PIA) of 20 h at 400 °C.
机译:在Fe-0.8 AT中研究了锰添加对形成富铜沉淀物的初始阶段的影响。%Cu(VH)和Fe-0.78。%Cu-1.05%Mn(Vd)模型合金中子照射到低流量。这些实验是先前的原子探测断层扫描(APT)和小角度中子散射(SAN)对这些模型合金的表征的延续。在先前的研究中,这些合金的中子被照射到10×10〜(23)n m〜( - 2)(e> 1 mev)[1]的流量。在这些新实验中,VH和VD合金在温度为288°的温度下照射到4×10〜(21)Nm〜(-2)和5×10〜(22)Nm〜(-2)的流量较低的中子C。在400℃的后照射退火(PIA)后,还检查辐照为5×10〜(22)n m〜(-2)的流量的试样。

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