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Investigations on thermal stresses of a graded Ti(C,N) coating deposited on WC-Co hardmetal

机译:WC-Co Hardutal沉积的分级Ti(C,N)涂层的热应力的研究

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We investigated the stress behaviour of Ti(C,N) coatings deposited on WC-Co substrates during an individual thermal cycle. The stress analyses were performed in-situ by energy dispersive X-ray diffraction using a white synchrotron beam. The stresses were determined using the sin~2 ψ method combined with scattering vector measurements at the strain-free ψ-tilt, in order to avoid the effect of the chemical C/N gradient on the strain distributions over sin~2 ψ. It was found that compressive stresses induced by top blasting on the coating are released after the individual thermal cycle. During heating and cooling, part of the Ti(C,N) coating was oxidized into a TiO_2 rutile phase. Stress analysis was also performed in this phase in order to evaluate the influence of oxidation on the residual stress of the coating. The obtained results can support the design of coated tools with improved properties at interrupted cutting operations by understanding the role of thermal cycling on the stresses of Ti(C,N) coatings.
机译:我们研究了在单独的热循环期间沉积在WC-CO基质上的Ti(C,N)涂层的应力行为。使用白色同步梁束通过能量分散X射线衍射原位进行应力分析。使用SIN〜2℃的方法确定应力与散射矢量测量结合在无应变ψ倾斜中,以避免化学C / N梯度对SIN〜2°的应变分布的影响。结果发现,在单个热循环之后释放通过涂层上的顶部爆破引起的压缩应力。在加热和冷却过程中,将部分Ti(C,N)涂层氧化成TiO_2金红石相。在该阶段还进行应力分析,以评估氧化对涂层残余应力的影响。通过了解热循环对Ti(C,N)涂层的应力的作用,所获得的结果可以支持具有改进性能的涂层工具的设计。

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