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DETERMINATION OF ALIGNMENT ERRORS IN CLASSICAL XRD RESIDUAL STRESS METHODS

机译:经典XRD残余应力方法中对准误差的测定

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The applicability of a recently introduced method will be discussed for the determination and -software- correction of alignment errors in XRD residual stress methods. For residual stress measurements with the omega-offset method the equatorial beam misalignment and the specimen displacement are relevant and the axial beam misalignment can be ignored. With the psi-tilt method the axial beam misalignment and the specimen displacement are relevant and the equatorial beam misalignment can be ignored. The two relevant alignment errors can be determined independently even when both errors are present. The method allows a free choice for the material of the stress-free reference sample. Each alignment error is described with only one distance parameter independent from the diffraction angle investigated or tilt angle applied. Hence, the alignment errors can be determined at one diffraction angle and applied over the complete 2θ range and other tilt angles than used for the determination of the errors. This will be demonstrated with measurements in the psi-stress set-up. The analysis and software correction of alignment errors makes the result fully independent of the alignment condition of the instrument. It allows comparison of stress results obtained in different laboratories and it is therefore a valuable addition to the international normalization procedure for XRD residual stress measurements.
机译:将讨论最近引入的方法的适用性,用于XRD残余应力方法中的对准误差的确定和贵文校正。对于利用ω-偏移方法的残余应力测量,赤道梁未对准和样本位移是相关的,并且可以忽略轴向梁未对准。利用PSI-倾斜法,轴向梁未对准和样本位移是相关的,并且可以忽略赤道梁未对准。即使存在两个错误,也可以独立地确定两个相关的对准误差。该方法允许对不含应力参考样品的材料自由选择。每个对准误差仅用一个距离参数描述,无关,该距离参数独立于所施加的衍射角或倾斜角度。因此,可以在一个衍射角处确定对准误差并在完整的2θ范围内施加而不是用于确定误差的完整2θ范围和其他倾斜角度。这将在PSI-ressult设置中进行测量。对准误差的分析和软件校正使得结果完全独立于仪器的对准状态。它允许比较在不同实验室中获得的应力结果,因此对于XRD残余应力测量的国际归一化程序是有价值的。

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