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Post-heat Treatment Effect on the Dielectric Response of Epoxy Samples

机译:热处理效应对环氧样品的介电响应

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In the present experiment, the dielectric response of various types of epoxies was investigated in the frequency and time domain. The samples consisted of nanostructured epoxy microcomposites and reference microcomposites. Water ingression at the fabrication step and/or at measuring time is known to affect the dielectric response of materials such as epoxy. Prior to measurement, some samples were submitted to 160°C during 48 hours under vacuum. Heating the epoxy sample under vacuum was found to have a substantial effect on dielectric properties specially when the microcomposite was nanostructured. In the nanodielectric case, pre-treatment conditions could produce a drop in the dielectric constant, about 5% at around 10~(-2) Hz. This observation would be consistent with the removal of the polarisability associated with water molecules.
机译:在本实验中,在频率和时域中研究了各种类型环氧树脂的介电响应。样品由纳米结构环氧微孔复合材料和参考微孔复合材料组成。已知制造步骤和/或在测量时间处的水进入以影响诸如环氧树脂的材料的介电响应。在测量之前,在真空下在48小时内将一些样品提交至160℃。发现在真空下加热环氧样品在微型复合材料是纳米结构时特别对介电性质具有显着影响。在纳米二电壳体中,预处理条件可以产生介电常数下降,约5%在10〜(-2)Hz。该观察结果与去除与水分子相关的可极化性一致。

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