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Corrosion behavior of additively manufactured 304 stainless steel in acidic media

机译:在酸性介质中腐蚀性制造的304不锈钢的腐蚀行为

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Additive manufacturing has recently begun to emerge as an important commercial manufacturingtechnology due to directly fabricate and repair complex metallic components that reduce theprocessing time and costs compared with traditional methods. However, the corrosion behavior ofadditively manufactured (AM) alloys has been sparsely studied and very little work has beenpublished so far. Corrosion will remain an important aspect needed to be treated for AM alloys.Therefore further research in terms of microstructure characterization and corrosion testing isrequired. Thus, the objective of this work is to study the corrosion response of AM 304 stainlesssteel (SS) in acidic solutions. The wrought counterpart was used to make the comparison. Firstly,the AM 304 SS specimen was produced using an AM-250 unit with a powder particle size in therange of 15-50 um. The microstructure of AM 304 SS was characterized by utilizing EDS, XRD,SEM instruments. The chemical composition and fine microstructure of the passive film on AM304 SS and wrought counterpart in acidic solution were characterized by XPS. The corrosionbehaviors of the passive film on two kinds of specimens were evaluated by electrochemicalanalysis. The dependence for the occurrence of faradic and non-faradic reactions on the nature ofthe passive film was investigated by EIS. The corrosion current density (i_(corr)) and breakdownpotential of passive film on specimens was revealed by cyclic polarization tests. Finally, theintegrated barrier characteristics of AM SS in acidic solution was evaluated and compared with thecounterpart.
机译:添加剂制造最近开始成为重要的商业制造业 技术由于直接制造和修复减少复杂金属组件的技术 处理时间和成本与传统方法相比。但是,腐蚀行为 含有薄荷的(am)合金已经稀疏地研究,并且工作很少 到目前为止发布。腐蚀仍然是艾合金需要治疗所需的一个重要方面。 因此,在微观结构表征和腐蚀测试方面进一步研究是 必需的。因此,这项工作的目的是研究AM 304不锈钢的腐蚀响应 钢(SS)在酸性溶液中。锻造的对应物用于进行比较。首先, AM-250单元使用粉末粒径的AM-250单元生产AM-250 SS样本。 范围为15-50 um。通过利用EDS,XRD,AM 304 SS的微观结构的特征在于, SEM仪器。 am上被动膜的化学成分和细胞微观结构 XPS的特征在于酸性溶液中的304 ss和锻造对应物。腐蚀 通过电化学评估两种样品的被动膜的行为 分析。对Faradic和非法反应发生的依赖性 通过EIS研究了无源胶片。腐蚀电流密度(i_(corr))和故障 循环偏振试验揭示了样品上被动膜的潜力。最后, 评估酸性溶液中AM SS的集成屏障特性并与 对方。

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    ZHIJUN ZHENG;

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