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Response Surface Design for Cellulose Production from Water Hyacinth to Synthesize Sodium Carboxymethyl Cellulose

机译:水葫芦纤维素生产的响应面设计从羧甲基纤维素合成羧甲基纤维素

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Eichhornia crassipes of water hyacinth is a waterweed in Thailand and cause an environmental problem. However, the biochemical in biomass especially cellulose can be utilized as substrate for biochemical production. This research aims to investigate the optimal system for extracting alpha cellulose from water hyacinth by using response surface experimental design, and then synthesize carboxymethyl cellulose (CMC). The results show that solid-to-liquid ratio significantly increase alpha-cellulose yield (p < 0.05) rather than NaOH concentration and contact time. The optimal condition is one g of dried water hyacinth with 17.25 mL of 4.89%(w/v) of NaOH solution for 3 hours under 70°C, can yield 81.4% of alpha-cellulose in total extracted cellulose weight. Comparing the properties of water hyacinth CMC (WH-CMC) with commercial CMC (C-CMC), we found that the moisture content and the degrees of substitution of C-CMC were higher than WH-CMC, but the purity was lower than WH-CMC from cellulose that not bleached with hydrogen peroxide (unbleach WH-CMC). Unbleach WH-CMC are propably comparable with C-CMC.
机译:水葫芦的Eichhornia褶皱是泰国的水藻,导致环境问题。然而,尤其是纤维素的生物化学中的生物化学可以用作生物化学生产的基质。本研究旨在通过使用响应表面实验设计来研究从水葫芦中提取α纤维素的最佳系统,然后合成羧甲基纤维素(CMC)。结果表明,固液比显着增加α-纤维素产率(P <0.05)而不是NaOH浓度和接触时间。最佳条件是1克干燥的水葫芦,17.25ml 4.89%(w / v)的NaOH溶液在70℃下3小时,可以在总提取的纤维素重量中产生81.4%的α-纤维素。与商业CMC(C-CMC)的水葫芦CMC(WH-CMC)的性质进行比较,我们发现水分含量和C-CMC的取代度高于WH-CMC,但纯度低于WH -CM来自未与过氧化氢漂白的纤维素(未漂白WH-CMC)。解开WH-CMC可与C-CMC相当。

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