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Removal of VOCs with TPF and TNPF Prepared by Electrospinning

机译:用电纺丝制备的TPF和TNPF去除VOC

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Titanium Nanotube (TNT) used in this study was prepared by a modified hydrothermal method, using a mixture of Titania Degussa P-25 (TiO_2), sodium hydroxide and deionized water as a solvent. In this study, the photocatalysts fibers were prepared by electrospinning under 20 kilovolts (kV) at a distance of 15 centimeter (cm). TiO_2and TNT were mixed with polyvinyl alcohol (PVA) to generate TiO_2 photocatalysts fibers (TPF) and TNT photocatalysts fibers (TNPF), respectively. The physical and chemical properties of the photocatalysts were indicated with spectrophotometer (UV-vis), X-ray diffractometer (XRD), Fourier-Transformed Infrared Spectrometer (FTIR), Thermogravimetric Analyzer (TGA), and Scanning Electron Microscope (SEM) characterization instruments. A single factor experimental method was used to investigate the effects of operational parameters, such as initial concentration and retention time and light source, on acetone removal performance with TPF and TNPF. The results showed that the degradation efficiency increased with increasing initial concentrations. The acetone removal efficiency was greater than 90% under a retention time above 40 seconds; initial acetone concentration of less than 1,000 parts per million (ppm); and ultraviolet (UV) light source of 365 nanometer (nm)with TPF. In addition, the efficiency was greater than 90%under a retention time of above 100 seconds; initial acetone concentration of less than 500 ppm; and UV light source of 365 nm with TNPF.
机译:本研究中使用的钛纳米管(TNT)是通过改良的水热法制备的,使用Titania Degussa P-25(TiO_2),氢氧化钠和去离子水的混合物作为溶剂。在这项研究中,光催化剂纤维是通过在15厘米(cm)的距离下在20 kV(kV)下静电纺丝制备的。将TiO_2和TNT与聚乙烯醇(PVA)混合,分别生成TiO_2光催化剂纤维(TPF)和TNT光催化剂纤维(TNPF)。用分光光度计(UV-vis),X射线衍射仪(XRD),傅立叶变换红外光谱仪(FTIR),热重分析仪(TGA)和扫描电子显微镜(SEM)表征仪器指示光催化剂的物理和化学性质。 。采用单因素实验方法研究了操作参数(如初始浓度,保留时间和光源)对TPF和TNPF去除丙酮性能的影响。结果表明,降解效率随初始浓度的增加而增加。在超过40秒的保留时间下,丙酮的去除效率大于90%;丙酮的初始浓度小于1,000 ppm(ppm);以及带有TPF的365纳米(nm)的紫外(UV)光源。此外,在100秒以上的保留时间下,效率大于90%。丙酮的初始浓度小于500 ppm;和TNPF的365 nm紫外光源。

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