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MECHANICAL CHARACTERISTICS OF AN ANODIZED MAGNESIUM ALLOY FOR BIODEGRADABLE IMPLANTS

机译:可生物降解植入物阳极化镁合金的力学特性

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In recent years, magnesium (Mg) alloys have emerged as possible biodegradable implant materials; however the degradation rate of Mg occurs at a higher rate than tolerable for the human body. Plasma electrolytic oxidation (PEO) has been used in the past as a useful surface treatment technique to improve the anti-corrosion properties of Mg alloys by forming protective coatings. This present work focuses on the effect of electrolyte solution on the corrosion, microstructural, and nanomechanical behavior of PEO coatings for possible use in biodegradable implants. The experimental parameters applied during PEO process did influence the structure, thickness, and morphology of the coating. Microstructural characterization of the coating was carried out by X-ray diffraction (XRD), scanning electron microscopy (SEM) followed by image analysis and energy dispersive spectroscopy (EDX). Further, nanoindentation was employed to evaluate nanohardness and Young's modulus of the PEO coating. The results show beneficial effects of the PEO coating to enhance the corrosion resistance of the uncoated AZ31 magnesium alloy. The XRD pattern shows that the components of the film vary based on electrolyte solution. The film composition does affect the nanomechanical behavior.
机译:近年来,镁(Mg)合金已成为可能的可生物降解的植入物材料。但是,Mg的降解率高于人体所能忍受的速率。过去,等离子体电解氧化(PEO)作为一种有用的表面处理技术,通过形成保护性涂层来改善Mg合金的防腐性能。这项工作的重点是电解质溶液对可用于可生物降解植入物的PEO涂层的腐蚀,微观结构和纳米力学行为的影响。 PEO过程中使用的实验参数确实影响了涂层的结构,厚度和形态。涂层的微观结构表征是通过X射线衍射(XRD),扫描电子显微镜(SEM),图像分析和能量色散光谱(EDX)进行的。此外,采用纳米压痕法评价PEO涂层的纳米硬度和杨氏模量。结果表明,PEO涂层对增强未涂层的AZ31镁合金的耐腐蚀性具有有益的作用。 XRD图谱表明,膜的成分根据电解质溶液而变化。膜的组成确实会影响纳米机械性能。

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