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PRODUCTION OF CAST AZ91-CNT NANO-COMPOSITE BY ADDITION OF Ni-P-CNT COATED MAGNEIUSM POWDER TO THE MELT

机译:Ni-P-CNT包覆的镁粉熔体的熔铸法生产AZ91-CNT纳米复合材料

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High agglomeration tendency and poor wettability of CNTs with metallic matrices are the main challenges for using this unique material as the reinforcement in magnesium based composites. In this study, nickel- phosphorous electroless coating process was employed for uniform co-deposition of CNTs into the Ni-P coating on the magnesium powder for the first time. The magnesium powder with the optimum composite coating was then used as the reinforcement and was introduced into the molten AZ91 alloy using stir casting method. Similar composites were also produced with untreated as-purchased CNTs for comparison. It was observed that addition of CNTs dispersed in the electroless coating resulted in refinement of the grain size, reduction in the porosity content and improvement of the hardness and flexural strength. Untreated CNTs were not able to improve the structural and mechanical characteristics of the cast composites to the same extent. This is believed to be due to the more agglomeration, less uniform distribution and poor wettability of the untreated CNTs with the melt compared to those introduced to the melt through the Mg-Ni-P-CNT composite powder.
机译:使用这种独特的材料作为镁基复合材料中的补强材料,CNT的高附聚趋势和较差的润湿性是金属基质的主要挑战。在这项研究中,首次采用镍-磷化学镀工艺将碳纳米管均匀共沉积到镁粉上的镍-磷涂层中。然后将具有最佳复合涂层的镁粉用作增强材料,并采用搅拌铸造法将其引入熔融的AZ91合金中。还用未经处理的购买的碳纳米管生产了类似的复合材料,以进行比较。观察到,分散在无电涂层中的CNT的添加导致晶粒尺寸的细化,孔隙率含量的降低以及硬度和抗弯强度的提高。未经处理的碳纳米管不能在相同程度上改善铸塑复合材料的结构和机械特性。据信这是由于与通过Mg-Ni-P-CNT复合粉末引入到熔体中的那些相比,未处理的CNT与熔体的附聚性更高,分布更不均匀并且润湿性差。

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