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Oxidation and gamma prime particle coarsening behavior of in-738 and GTD-111

机译:In-738和GTD-111的氧化和γ′粒子粗化行为

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Cyclic oxidation and long-term isothermal exposure tests were conducted on GTD-111 and IN-738 alloys to evalaute the variation of oxidation and gamma prime particle coarsening bheavior between these alloys. Cyclic oxidation behavior of these alloys was compared by plotting the weigth change of the test specimens as a function of thermal cycles. The results showed that GTD-111 was less resistnat to oxidation compared to IN-738. To characterize oxide scale, short-term isothermal oxidation tests were conducted at two temperatures, and spalled oxide was collected and analyzed by EDS as a function of aging. The composition of the oxide varied between the materials. The long-term exposure tests (up to 10,000 hours) were conducted at four temperatures to assess gamma prime particle coarsening behavior. Metallographic work was performed on both the cyclic oxidation and isothermally aged samples to characterize oxidation attack and gamma prime coarsening as a function of aging time and thermal cycles. At all aging temperatures and/or times investigated, the gamma prime particles in the GTD-111 specimens were coarser than in IN-738. The variation of the oxidation and the gamma prime coarsening behavior between these alloys is discussed in terms of chemistry differences between IN-738 and GTD-111.
机译:在GTD-111和IN-738合金上进行了循环氧化和长期等温暴露测试,以评估这些合金之间的氧化变化和γ初生颗粒粗化行为。通过绘制测试样品的重量变化随热循环变化的曲线,比较了这些合金的循环氧化行为。结果表明,与IN-738相比,GTD-111对氧化的抵抗力较小。为了表征氧化物垢,在两个温度下进行了短期等温氧化试验,收集了剥落的氧化物,并通过EDS进行了老化分析。氧化物的组成因材料而异。在四个温度下进行了长期暴露测试(长达10,000小时),以评估γ质颗粒的粗化行为。在循环氧化和等温时效样品上均进行了金相研究,以表征随着时效时间和热循环而发生的氧化腐蚀和伽马素粗化。在研究的所有老化温度和/或时间下,GTD-111样品中的γ初粒子比IN-738中的更粗。根据IN-738和GTD-111之间的化学差异,讨论了这些合金之间的氧化变化和γ素粗化行为。

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