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Synthesis of Silver Nanoparticles Using Tyrosine as Reductor and Capping Agent

机译:使用酪氨酸作为还原剂和封盖剂的合成银纳米粒子

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Synthesis and stability of silver nanoparticles (AgNPs) using tyrosine as a reducing and capping agent have been done. Synthesis of AgNPs was performed by mixing silver nitrate (AgNO_3) solution as a precursor with tyrosine amino acid and heating it in a boiling water bath until characterized by the appearance of color change from colorless to yellow. Variations in pH, concentration, and reaction time affecting the formation of AgNPs were studied using UV-Vis spectrophotometry in the wavelength range of 300-700 nm as the main device. The synthesis was successfully conducted at pH 11 for 45 min with the optimum tyrosine concentration was 3 mM for 0.5 mM AgNO_3. The optimum mole ratio AgNO_3 0.5 mM to tyrosine 3 mM was 1:6. TEM and PSA characterizations showed that the particle was a round shape and 29.5 nm is average size, respectively.
机译:已经完成了使用酪氨酸作为还原剂和封端剂的银纳米颗粒(AgNP)的合成和稳定性。通过将硝酸银(AgNO_3)溶液混合为具有酪氨酸氨基酸的前体并将其加热在沸水浴中来进行AgNP的合成,并通过从无色至黄色的颜色变化的外观表征。使用300-700nm的波长范围为主装置,研究了影响影响AgNP的形成的pH,浓度和反应时间的变化。合成在pH 11在pH 11成功进行45分钟,最佳酪氨酸浓度为3mm,0.5mM AgNO_3。酪氨酸3mm的最佳摩尔比AgNO_3 0.5mm为1:6。 TEM和PSA表征表明,颗粒是圆形,分别为29.5nm是平均尺寸。

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