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The Influence of Thermomechanical Processing on the Microstructure of Particu-late Reinforced Titanium Metal Matrix Composites

机译:热机械加工对颗粒增强钛金属基复合材料微观结构的影响

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Ti and Ti-6A1-4V matrix composites reinforced with 5%, 10%, 15% and 20%vol. particulate TiC were prepared using two powder metallurgy routes. The composites were either sintered at 1375°C or hot pressed at 920°C under argon atmosphere. Both methods were followed by hot deformation with strain rates ranging from 0. 001s-1 to 0. 1s-1 and temperature varying from 850°C to 1050°C. The microstructures of the composites were examined by scanning electron microscopy (SEM) coupled with electron backscattering diffraction (EBSD). The density,grain size and volume fractions of the phases were measured from these observations. Complete densification of this type of composite cannot be achieved by sintering alone. Furthermore,at high temperatures,TiC reacts with metal Ti and transforms progressively into TiC0.5. However,by hot pressing the composite powder.it was possible to obtain fully dense composites with a finer micnistructure and to limit the reaction between TiC and Ti. The objective of the forging step is to suppress the remaining porosity and refine the manostructure to increase the mechanical properties of the composites. This study proposes a method to identify the best forging parameters for vorious configurations (grain size, reinforcement volume fraction,matrix nature) of titanium matrix reinforced with particulate TiC.
机译:以5%,10%,15%和20%vol增强的Ti和Ti-6A1-4V基复合材料。使用两种粉末冶金方法制备了颗粒状的TiC。将该复合物在氩气气氛下于1375℃下烧结或在920℃下热压。两种方法之后都是热变形,应变速率从0. 001s-1到0. 1s-1,温度从850°C到1050°C不等。通过扫描电子显微镜(SEM)结合电子背散射衍射(EBSD)检查了复合材料的微观结构。从这些观察值测量相的密度,粒度和体积分数。这种类型的复合材料的完全致密化不能仅通过烧结来实现。此外,在高温下,TiC与金属Ti反应并逐渐转变为TiC0.5。但是,通过热压复合粉末,可以获得具有更细微结构的完全致密的复合材料,并限制了TiC和Ti之间的反应。锻造步骤的目的是抑制残留的孔隙率并细化Manostructure,以提高复合材料的机械性能。这项研究提出了一种方法来确定最佳的锻造参数,该参数是用颗粒TiC增强的钛基体的涡旋构型(晶粒尺寸,增强体体积分数,基体性质)的最佳选择。

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