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Preparation and Characterization of Coated Carbon Black Pigment

机译:涂层炭黑颜料的制备与表征

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Black pigment is an important pigment in the ceramic decoration. The traditional black pigment is spinel type matter containing Co, Fe or Cr elements. Carbon black is the best black pigment and is nontoxic. However, carbon black is oxygenated in the ceramic sintering process at atmosphere. Carbon black enclosed in the crystal latter of ZrSiO_4 was reported. However, the content of carbon black is little which decreases the color generation. Carbon black coated with SiO_2 was prepared by sol-gel method using combustion method using SiO_2 sol and black ink as raw materials. The obtained black pigment was characterized by XRD, TEM and ultraviolet-visible spectrophotometer. The results show that the black pigment does not change its color after calcinations at 1300 °C at atmosphere implying the carbon black is coated completely with SiO_2.
机译:黑色颜料是陶瓷装饰中的重要颜料。传统的黑色颜料是含有Co,Fe或Cr元素的尖晶石型物质。炭黑是最好的黑色颜料,无毒。但是,炭黑在大气中的陶瓷烧结过程中被氧化。据报道,在ZrSiO_4的晶体后面封入了炭黑。然而,炭黑的含量很少,这降低了颜色的产生。以SiO_2溶胶和黑色墨水为原料,采用燃烧法通过溶胶-凝胶法制备了涂覆有SiO_2的炭黑。用XRD,TEM和紫外可见分光光度计对所得黑色颜料进行表征。结果表明,在1300°C的气氛下煅烧后,黑色颜料不会改变其颜色,这意味着炭黑完全被SiO_2覆盖。

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