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Preparation and Properties of Nano-hydroxyapatite Derived from Sol-gel Method for Cu~(2+) Polluted Water

机译:溶胶-凝胶法制备Cu〜(2+)污染纳米羟基磷灰石及其性能

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Nano-hydroxyapatite (HAP) was prepared by sol-gel method with Ca(NO_3)2·4H_2O and H3PO4 precursors. The result was shown that the powder was spherical with very little reunion and the particle size was around 50nm. The HAP adsorbent was utilized for copper removal from aqueous solutions using the batch technique. Some parameters that determine copper ion uptake including contact time, adsorbent dose, the solution temperature and initial concentration of the copper in the aqueous solution were evaluated. The experimental results showed that a better removal efficiency was about 99.27 % at pH 7, 40°C, contact time 60 min, adsorbent dose of 5 g/L and initial concentration of 60 mg/L.
机译:以Ca(NO_3)2·4H_2O和H3PO4为前驱体,通过溶胶-凝胶法制备了纳米羟基磷灰石(HAP)。结果表明,该粉末是球形的,具有很少的团聚,并且粒径为约50nm。使用分批技术将HAP吸附剂用于从水溶液中去除铜。评价了决定铜离子吸收的一些参数,包括接触时间,吸附剂剂量,溶液温度和水溶液中铜的初始浓度。实验结果表明,在pH 7、40°C,接触时间60分钟,吸附剂剂量为5 g / L和初始浓度为60 mg / L时,较好的去除效率约为99.27%。

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