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Surface Modification and Preparation of High Purity Nanometer Magnesium Hydroxide Using Impinging Stream

机译:撞击流法制备高纯纳米氢氧化镁。

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High purity nanometer magnesium hydroxide is produced by impinging stream reaction crystallization method using bischofite as feedstock. Effects of operation conditions on the impinging stream of Mg (OH)_2 are reported and the control factors of purity are confirmed. The morphology of the powder was characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Result shows that purity of Mg (OH)_2 can reach 99% and the mean size of crystal is 13.5nm. Surface modification of nano-sized magnesium hydroxide using four surface modifiers such as sodium steatite, sodium laurylsulfonate, sodium oleate and sodium silicate were investigated in this paper. The modified magnesium hydroxide has smaller particle size, larger powder contact angle, slower sedimentation velocity, the less in-oil capacity than unmodified sample
机译:采用重水铁矿为原料,通过冲击流反应结晶法制备了高纯度的纳米氢氧化镁。报道了操作条件对Mg(OH)_2撞击流的影响,并确定了纯度的控制因素。通过X射线衍射(XRD)和透射电子显微镜(TEM)表征粉末的形态。结果表明,Mg(OH)_2的纯度可达到99%,晶体平均尺寸为13.5nm。本文研究了使用滑石酸钠,十二烷基磺酸钠,油酸钠和硅酸钠等四种表面改性剂对纳米氢氧化镁进行的表面改性。与未改性样品相比,改性氢氧化镁具有较小的粒径,较大的粉末接触角,较慢的沉降速度和较小的油内容量

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