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Optimizing operating parameters of spectrophotometer for testing transmission spectrum of optical substrate

机译:优化分光光度计的工作参数以测试光学基板的透射光谱

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The optical characteristics of substrates are the essential content of research work for thin film optics. The spectrophotometer is one of the important instruments to test transmittance and reflectance of different substrates or coating components. The test accuracy of transmission spectrum of the substrates has direct influenced on optical constants reverse engineering of thin film on the substrate. In this paper, SCHOTT grade LITHOSIL_Q0 fused silica substrate was chosen as standard substrate and was tested transmission spectrum in region 380nm-860nm to use the Lambda-900 spectrophotometer. By comparing the measured transmission spectrum with standard SCHOTT grade LITHOSIL_Q0 fused silica substrate transmission spectrum can be calculated measured errors. In the experiments, the orthogonal experimental design method is used. Sample pool aperture, scan speed, slit width and sampling data interval operating parameters were chosen as key factors (three levels were chosen in each factor). L_9 (3~4) orthogonal table was used for analysis the experiments results. Nine experiment results analyzed to determine the operating parameters of the influence measured accuracy were as follows: the sample pool aperture, scan speed, slit width, the sampling data interval. Finally, no iris, scan speed 250nm/s, slit width 3nm, sampling data interval lnm were used a combination of the operating parameters to measure of transmission spectrum of the SCHOTT grade LITHOSIL_Q0 samples. Measured maximum and minimum absolute error are 0.1355% and 0.0771%, respectively. The operating parameters could be applied to transmittance spectrum test of every substrate, or the spectrum could be extended.
机译:基板的光学特性是薄膜光学研究工作的基本内容。分光光度计是测试不同基材或涂料组分的透射率和反射率的重要仪器之一。基板透射光谱的测试精度直接影响光学常数,对基板上的薄膜进行逆向工程。本文选择SCHOTT等级的LITHOSIL_Q0熔融石英基板作为标准基板,并使用Lambda-900分光光度计测试了380nm-860nm区域的透射光谱。通过将测得的透射光谱与标准SCHOTT级LITHOSIL_Q0熔融石英基材的透射光谱进行比较,可以计算出测量误差。在实验中,使用正交实验设计方法。选择样品池孔径,扫描速度,狭缝宽度和采样数据间隔操作参数作为关键因素(每个因素中选择了三个级别)。用L_9(3〜4)正交表对实验结果进行分析。分析九个实验结果,确定对运行参数的影响,测量精度的影响分别为:样品池孔径,扫描速度,狭缝宽度,采样数据间隔。最后,没有虹膜,扫描速度为250nm / s,缝隙宽度为3nm,采样数据间隔为1nm,结合了操作参数来测量SCHOTT级LITHOSIL_Q0样品的透射光谱。测得的最大和最小绝对误差分别为0.1355%和0.0771%。可以将操作参数应用于每个基板的透射光谱测试,或者可以扩展光谱。

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