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A study on failure of double-layer thermal barrier coatings subjected to uniaxial compression tests using acoustic emission analysis and digital image correlation

机译:使用声发射分析和数字图像相关性对单轴压缩试验进行双层热阻挡涂层失效的研究

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The failure behavior and fracture process of double-layer thermal barrier coatings under uniaxial compressive substrate loading has been investigated. Coating systems containing GZO with low and high porosity (LP, HP) were fabricated to examine the influence of microstructure on failure behavior and strain energy. An YSZ-HP single-layer system serves as a reference. All ceramic coatings were deposited via atmospheric plasma spraying (APS) on cylindrical rods and turbine blade-shaped specimens made from CoNiCrAlY (LCO-22) coated, nickel-based, single crystal superalloy (PWA 1483). Prior to compression tests, isothermal pre-oxidation at 1050°C and dwell-times of 100, 500 and 1.500 hours, as well as cyclic annealing tests between 50 and 1050°C up to 500 cycles were performed, to study the effects of thermal ageing on strain energy to failure. In-situ acoustic emission (AE) measurements provides quantitative information about the failure processes under compressive substrate loading. A stereo camera system monitors the three-dimensional displacements and the surface fracture processes. For as-sprayed coatings, strain to failure of the investigated GZO/YSZ systems is comparable to the referenced single-layer TBC. AE analysis indicates coating failure at earlier stages and less substrate loads after thermal ageing with increasing dwell-time. Consequently, the pre-oxidation leads to reduced strain to failure values in all investigated coating systems. Digital image correlations (DIC) suggests that the failure behavior of as-sprayed GZO/YSZ coatings is similar to the referenced YSZ system. However, a different behavior was observed for pre-oxidized coatings, where cracking and spallation of GZO occurs predominantly.
机译:研究了单轴压缩基材负载下双层热阻挡涂层的故障行为和断裂过程。制备含有低孔隙率和高孔隙率(LP,HP)的GZO的涂层系统,以检查微观结构对失效行为和应变能的影响。 YSZ-HP单层系统用作参考。所有陶瓷涂层通过圆柱形杆和汽轮机叶片形样品上的大气等离子体喷涂(AP)沉积,由Conicraly(LCO-22)涂覆的镍基单晶超合金(PWA 1483)上制成。在压缩试验之前,1050℃的等温预氧化和100,500和1.500小时,以及50-1050℃的循环退火测试,高达500个循环,以研究热量的影响对应变能量的衰老失败。原位声发射(AE)测量提供关于压缩基板负载下的故障过程的定量信息。立体声摄像机系统监控三维位移和表面骨折过程。对于喷雾涂层,研究的GZO / YSZ系统的菌株与参考单层TBC相当。 AE分析表明热老化后较早阶段和较少的基板负载,随着停留时间的增加而较少的基板负载。因此,预氧化导致所有研究的涂料系统中的失效值减少。数字图像相关性(DIC)表明,喷涂的GZO / YSZ涂层的故障行为类似于引用的YSZ系统。然而,对于预氧化涂层观察到不同的行为,其中GZO的开裂和脱落主要发生。

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