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Comparative Analysis of Adding Hydrogen Peroxide or Ethanol in Preparation of Zirconia Nano-Powder by Coprecipitation Methods

机译:共沉淀法制备氧化锆纳米粉体中添加过氧化氢或乙醇的比较分析

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Zirconia precursor was prepared by adding hydrogen peroxide or ethanol in co-precipitation process from raw materials of ZrOC12·8H2O and ammonia,the zirconia powders were subsequently obtained by calcination of the precursor at 600 °C and ball milling.Through the analyzed by TG-DTA,XRD,SEM,the results show that by adding hydrogen peroxide or ethanol in co-precipitation process can reduce the produce of agglomerate.Ethanol and hydrogen peroxide addition on zirconia by co-precipitation for different reaction results were compared and analyzed.
机译:在ZrOC12·8H2O和氨气的共沉淀过程中,通过共沉淀加入过氧化氢或乙醇制备氧化锆前驱体,然后在600°C下煅烧并球磨得到氧化锆粉末。 DTA,XRD,SEM结果表明,在共沉淀过程中加入过氧化氢或乙醇可以减少团聚体的产生。针对不同的反应结果,通过共沉淀在氧化锆上添加乙醇和过氧化氢进行了比较和分析。

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