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Comparative Analysis of Adding Hydrogen Peroxide or Ethanol in Preparation of Zirconia Nano-Powder by Coprecipitation Methods

机译:共沉淀法制备氧化锆纳米粉体中添加过氧化氢或乙醇的比较分析

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摘要

Zirconia precursor was prepared by adding hydrogen peroxide or ethanol in co-precipitation process from raw materials of ZrOC_(12)·8U_2O and ammonia, the zirconia powders were subsequently obtained by calcination of the precursor at 600℃ and ball milling. Through the analyzed by TG-DTA, XRD, SEM, the results show that by adding hydrogen peroxide or ethanol in co-precipitation process can reduce the produce of agglomerate. Ethanol and hydrogen peroxide addition on zirconia by co-precipitation for different reaction results were compared and analyzed.
机译:在共沉淀过程中加入过氧化氢或乙醇,由ZrOC_(12)·8U_2O与氨共同制备氧化锆前驱体,然后在600℃煅烧并球磨得到氧化锆粉体。通过TG-DTA,XRD,SEM分析,结果表明,在共沉淀过程中加入过氧化氢或乙醇可以减少结块的产生。比较和分析了共沉淀法在氧化锆上加乙醇和过氧化氢的不同反应结果。

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  • 来源
    《Key Engineering Materials》 |2010年第2010期|793-795|共3页
  • 作者单位

    Faculty of Material and Metallurgical Engineering, Kunming University of Science and Technology, Kunming, Yunnan, 650093, PR China;

    rnFaculty of Material and Metallurgical Engineering, Kunming University of Science and Technology, Kunming, Yunnan, 650093, PR China;

    rnFaculty of Material and Metallurgical Engineering, Kunming University of Science and Technology, Kunming, Yunnan, 650093, PR China;

    rnFaculty of Material and Metallurgical Engineering, Kunming University of Science and Technology, Kunming, Yunnan, 650093, PR China;

    rnFaculty of Material and Metallurgical Engineering, Kunming University of Science and Technology, Kunming, Yunnan, 650093, PR China;

    rnFaculty of Material and Metallurgical Engineering, Kunming University of Science and Technology, Kunming, Yunnan, 650093, PR China;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    zirconia; hydrogen peroxide; coprecipitation; agglomeration;

    机译:氧化锆过氧化氢共沉淀凝聚;

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