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SrTiO3 Functional Ceramics Thin Film Prepared by Self-Assembled Monolayers with PTCS Substrate Functionalization

机译:SRTIO3功能陶瓷薄膜通过自组装单层制备,具有PTCS基板官能化

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This article used PTCS to dispose the self-assembled substrate,and prepared the precursor by the ratio of AHFT / SN / BA =1∶1∶3 and then immersed the functionalized substrate into the precursor supersaturated solution.With the colloidal particles absorption induced by SAMs,SrTiO3 thin film was prepared by the self-assembled monolayers with liquid phase deposition method.The effects of the time of UV radiation and the time of PTCS immersion on the substrate contact angle were studied and the time of UV radiation had an effect on the substrate functionalization after PTCS immersion.The results showed that the first UV radiation for 25 min,PTCS immersion for 7 min and the second UV radiation for 30 min were beneficial to the crystallization of SrTiO3.XRD and AFM were used to characterize the thin film physical phase and surface morphology at 600°Cwith annealing and heat retaining for 2 hours.The results also showed that under the same condition,the SrTiO3 crystals on the thin film surface had the clear outline and the spherical crystals were distributed regularly and evenly.
机译:本文使用PTC来设置自组装的基材,并通过AHFT / Sn / Ba = 1:1:3的比例制备前体,然后将官能化底物浸入前体过饱和溶液中。与胶体颗粒吸收SAMS,SRTIO3薄膜由具有液相沉积方法的自组装单层制备。研究了UV辐射时间的效果和PTCS浸没对基板接触角的影响,紫外线辐射的时间对PTCS浸渍后的基材官能化。结果表明,第一个UV辐射25分钟,PTCS浸渍7分钟,第二UV辐射30分钟对SRTIO3.XRD和AFM的结晶有益于薄膜600°Cwith退火和热保留2小时的物理相和表面形态。结果还表明,在相同的条件下,薄膜表面上的SRTIO3晶体有明确的轮廓,球形晶体定期分布。

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