首页> 外文会议>AME 2010;International conference on advanced mechanical engineering >Preparation and Characterization of Nanosized Barium-strontium Titanate Immobilized on Aluminum oxide and Its Application in Adsorption
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Preparation and Characterization of Nanosized Barium-strontium Titanate Immobilized on Aluminum oxide and Its Application in Adsorption

机译:氧化铝上固定的纳米钛酸锶锶钡的制备,表征及其在吸附中的应用

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Nanometer barium-stroutium titanate immobilized on aluminum oxide (ABST) was prepared by the citric acid sol-gel method and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared spectrophotometry (FTIR). Its Pb2+ and Cd2+ adsorption properties from water were studied. Adsorption and elution were investigated under different conditions. The results showed that the nanometer barium-strontium titanate was immobilized on aluminum oxide firmly, becoming a composite adsorbent. The lead and cadmium ions were quantitatively retained at pH 5-8; their adsorption capacities of ABST were 70.28 mg g-1 and 8.12 mg g-1, respectively. The adsorbent of adsorped lead and cadmium ions were regenerated completely by elution with 1 mol-L-1 HNO3. The adsorbent had a promising prospect in analyticl chemistry and water treatment.
机译:采用柠檬酸溶胶-凝胶法制备了固定在氧化铝(ABST)上的纳米钛酸钡锶,并通过X射线衍射(XRD),扫描电子显微镜(SEM)和傅里叶变换红外分光光度法(FTIR)对其进行了表征。研究了其在水中对Pb2 +和Cd2 +的吸附性能。在不同条件下研究了吸附和洗脱。结果表明,纳米钛酸锶钡牢固地固定在氧化铝上,成为复合吸附剂。铅和镉离子定量保留在pH 5-8;它们对ABST的吸附能力分别为70.28 mg g-1和8.12 mg g-1。用1 mol-L-1 HNO3洗脱可完全再生吸附的铅和镉离子的吸附剂。该吸附剂在分析化学和水处理方面具有广阔的前景。

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