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Preparation and performances of successive TiO2 thin film photocatalyst supported on carbon fiber

机译:碳纤维负载连续TiO2薄膜光催化剂的制备及性能

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Successive TiO2 film photocatalysts supported on surface modified PAN-carbon fiber (PAN-CF) substrates were prepared via the sol-gel dip-coating method with Ti(O4H9)4 as a precursor. Several techniques such as scanning electron microscope(SEM), thermogravimetric analysis (TGA), X-ray diffraction (XRD) were utilized to investigate the optimized concentrations of Ti sol, annealing temperature and their influence on the final properties of the TiO2/CF. The interfacial bonding properties of carbon fiber with TiO2 film was evaluated by ultrasonic vibration. The results show that M5TiO2/CF has favorable load fastness and load rate. The photocatalytic properties of TiO2/CF were investigated by degrading acid orange II (80mg/L) under UV irradiation. The results suggest that the catalytic activity have significant difference compared with M3TiO2/CF>M5TiO2/CF>M7TiO2/CF and the M5TiO2/CF has been shows the optimum catalytic performances.
机译:通过溶胶-凝胶浸涂法,以Ti(O4H9)4为前驱体,制备了负载在表面改性PAN-碳纤维(PAN-CF)基底上的TiO2薄膜光催化剂。利用扫描电子显微镜(SEM),热重分析(TGA),X射线衍射(XRD)等技术研究了钛溶胶的最佳浓度,退火温度及其对TiO2 / CF最终性能的影响。通过超声振动评价了碳纤维与TiO2薄膜的界面粘结性能。结果表明,M5TiO2 / CF具有良好的载荷坚牢度和载荷率。通过在紫外光下降解酸性橙II(80mg / L),研究了TiO2 / CF的光催化性能。结果表明,与M3TiO2 / CF> M5TiO2 / CF> M7TiO2 / CF相比,催化活性有显着差异,M5TiO2 / CF具有最佳的催化性能。

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